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Paper | Special issue | Vol 103, No. 2, 2021, pp.809-816
Published online, 19th January, 2021
DOI: 10.3987/COM-20-S(K)47
N-Glycosylation of Thio-glycoside Derived from Odorless Thiols Using Hypervalent Iodine(III) Reagent

Koji Morimoto, Kana Yanase, Tohru Kamitanaka, and Tetsuya Kajimoto*

*School of Pharmacy, Ritsumeikan University, 1-1-1 Noji-higashi, Kusatsu, Shiga, Japan

Abstract

A general and efficient protocol for direct N-glycosylation using inexpensive and readily available thioglycosides prepared from an odorless sulfur source was established. The use of easily available reactants and the mild reaction conditions make this protocol feasible for practical applications.