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Short Paper | Regular issue | Vol 98, No. 9, 2019, pp.1258-1264
Published online, 1st October, 2019
DOI: 10.3987/COM-19-14150
Electrooxidation of Chlorodiphenylphosphine under Ammonia Atmosphere. Synthesis of 2,2,4,4,6,6-Hexaphenylcyclotriphosphazene and Iminobis(aminodiphenylphosphorus) Chloride

Manabu Kuroboshi,* Yasunari Masumoto, and Hideo Tanaka

*Division of Chemsitry and Biochemistry, Graduate School of Natural Science and Technology, Okayama University, 3-1-1 Tsushima-naka, Okayama 700-8530, Japan

Abstract

Electrooxidation of MeCN solution of chlorodiphenylphosphine in the presence of Cl under NH3 atmosphere gave a mixture of 2,2,4,4,6,6-hexaphenylcyclotriphosphazene and iminobis(aminodiphenyl- phosphorus) chloride.