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Short Paper | Regular issue | Vol 94, No. 11, 2017, pp.2103-2110
Published online, 21st September, 2017
DOI: 10.3987/COM-17-13802
Synthesis and Crystal Structure of 4-Trifluoroacetyl-3-phenylsydnone

Masami Kawase,* Ryosuke Saijo, Shigeki Mori, and Hidemitsu Uno

*Faculty of Pharmaceutical Sciences, Matsuyama University, 4-2 Bunkyo-cho, Matsuyama, Ehime 790-8578, Japan

Abstract

4-Trifluoroacetyl-3-phenylsydnone was first synthesized by trifluoromethylation of 4-formyl-3-phenylsydnone followed by oxidation of the corresponding trifluoromethyl alcohol. The structure of the product was determined by single-crystal X-ray analysis.