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Obituary
Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Paper | Regular issue | Vol 94, No. 8, 2017, pp.1439-1455
Published online, 9th June, 2017
Published online, 9th June, 2017
DOI: 10.3987/COM-17-13726
■ Ultrasound-Mediated Three-Component Reaction “On-Water” Protocol For the Synthesis of Novel Mono- and bis-1,3-Thiazin-4-one Derivatives
Wael A. A. Arafa,* Ashraf M. Mohamed, and Ahmed F. Abdel-Magied
*Department Of Chemistry, Fayoum University, Fayoum 12975, Egypt
Abstract
Green synthetic and catalyst-free strategy towards the synthesis of novel mono- and bis-1,3-thiazin-4-one scaffolds through a one pot, reaction of carbon disulfide, monoacetylenic esters and amines under ultrasonication has been reported. The merits of this protocol comprise no need for tedious workup steps and afforded the desired products in excellent yields make this synthetic protocol more efficient and worthy of further attentiveness. Moreover, the method exhibited excellent score in a number of green metrics.
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