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Communication | Regular issue | Vol 89, No. 3, 2014, pp.627-630
Published online, 28th January, 2014
DOI: 10.3987/COM-13-12897
Synthesis and Characterization of Phenyl(1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-4-yl)methanone and Its Derivatives

Cong Liu, Rongji Dai,* Guowei Yao, and Yulin Deng*

*School of Life Science, Beijing Institute of Technology, 5 South Zhongguancun Street Beijing 100081, China

Abstract

A quick and highly efficient method for the synthesis of phenyl(1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecan-4-yl)methanone and its derivatives from hexamine and 2-bromo-1-arylethanones has been established via a Stevens rearrangement. Structures of the products were characterized by NMR and X-ray crystallography.