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■ Palladium-Catalyzed Mizoroki-Heck Type Reaction with Aryliodine Diacetates Using Hydrazone Ligand

Takashi Mino,* Kohei Watanabe, Taichi Abe, Taketo Kogure, and Masami Sakamoto

*Department of Applied Chemistry and Biotechnology, Graduate School and Faculty of Engineering, Chiba University, 1-33 Yayoi-cho, Inage-ku, Chiba 263-8522, Japan

Abstract

We developed a palladium-catalyzed Mizoroki-Heck type reaction of olefins with such hypervalent iodine reagents as iodobenzene diacetate in good to high yields using 2 mol% of a heterocyclic hydrazone (1b)-Pd(OAc)2 system in NMP under air at 90 °C.