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Communication | Special issue | Vol 88, No. 2, 2014, pp.961-968
Published online, 30th September, 2013
DOI: 10.3987/COM-13-S(S)95
■ No Catalyst, Radical Initiator and Photochemical Irradiation Approach to Direct α-Trifluoromethylation of Lithium Enolates

Yuichi Tomita, Toshiaki Iida, Ryota Hashimoto, Yoshimitsu Itoh, and Koichi Mikami*

*Department of Applied Chemistry, Graduate School of Science and Technology, Tokyo Institute of Technology, 2-12-1 Ookayama, Meguro-ku, Tokyo 152-8552, Japan

Abstract

Heterocyclic lactam lithium enolates exploit an access to the electrophilic radical α-trifluoromethylation without catalyst/radical initiator/photochemical irradiation.