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Obituary
Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Short Paper | Regular issue | Vol 87, No. 4, 2013, pp.897-908
Published online, 13th March, 2013
Published online, 13th March, 2013
DOI: 10.3987/COM-13-12678
■ Synthesis of 1,3-Dialkylperhydrobenzimidazolinium Salts and Their Catalytic Properties in Heck Reactions
Murat Yiğit,* Gülin Bayam, Beyhan Yiğit, and İsmail Özdemir
*Department of Chemistry, Faculty of Arts and Sciences, Adıyaman University, 02040 Adıyaman, Turkey
Abstract
Novel eight 1,3-dialkylperhydrobenzimidazolinium chloride salts 3a-h were prepared as precursors of N-heterocyclic carbenes by reacting N,N’-dialkylcyclohexandiamine, triethyl orthoformate and ammonium chloride. The salts were characterized spectroscopically and the complexes formed in situ from Pd(OAc)2 and 3 have been tested as catalysts in homogenous Heck coupling reactions.
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