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Communication | Special issue | Vol 79, No. 1, 2009, pp.359-364
Published online, 31st October, 2008
DOI: 10.3987/COM-08-S(D)30
Effective Synthesis of Optically Active 3-Phenyl-3-(3-trifluoromethyl)diazirinyl Bishomophenylalanine Derivatives

Yuta Murai, Yasumaru Hatanaka, Yuichi Kanaoka, and Makoto Hashimoto*

*Obihiro University of Agriculture and Veterinary Medicine, Inada-cho, Obihiro, Hokkaido 080-8555, Japan


Effective incorporation of phenyldiazirine moiety on the acyl residue of L- and D- glutamic acid by Friedel-Crafts reactions with triflic acid developed simple preparation of bishomophenylalanine (bhPhe) for aromatics, which added a versatile and a reliable access to photoreactive peptide probes.