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Communication | Special issue | Vol 5, No. 1, 1976, pp.339-345
Published online, 1st January, 1970
DOI: 10.3987/S-1976-01-0339
Hydroxyalkylation of N-Alkoxyquinaldinium and -lepidinium Perchlorates

Hiroshi Noda, Hisao Ekimoto, and Masatomo Hamana*

*Faculty of Pharmaceutical Sciences, Kyushu University, 3-1-1 Maidashi, Higashi-ku, Fukuoka 812-8582, Japan


Irradiation of N-alkoxyquinaldinium or -lepidinium perchlorate in alcohol affords 4- or 2-hydroxyalkylated methylquinoline and a small amount of 8-alkoxy-methylquinoline. Hydroxymethylation of the N-ethoxy salts occurs also homolytically in high yields on treatment with methanol and ammonium peroxydisulfate.