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Communication | Special issue | Vol 5, No. 1, 1976, pp.281-284
Published online, 1st January, 1970
DOI: 10.3987/S-1976-01-0281
Conversion of Caprolactam to Eight-membered Ene-lactam

Takeshi Oishi,* Mineo Fukui, Yoshio Ban, and Msanori Honda

*The Institute of Physical and Chemical Research, Wako-shi, Saitama 351-0198, Japan


Dichlorocarbene adduct of N-acetyl ketene-O,N-acetal(II) derived from caprolactam afforded the homologous ene-lactam on LiAlH4 reduction followed by base treatment.