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Communication | Regular issue | Vol 26, No. 6, 1987, pp.1467-1470
Published online, 1st January, 1970
DOI: 10.3987/R-1987-06-1467
New Methods and Reagents in Organic Synthesis. 68. Reaction of Thioketones with Lithium Trimethylsilyldiazomethane

Takayuki Shioiri, Yuji Iwamoto, and Toyohiko Aoyama

*Faculty of Pharmaceutical Sciences, Nagoya City University, Tanabe-dori, Mizuho-ku, Nagoya 467-8603, Japan


Reaction of thioketones with lithium trimethylsilyldiazomethane affords alkynes, vinylsilanes. 1,2,3-thiadiarolines, or 1,2,3-thiadiazoles depending upon substrates and reaction solvents.