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Communication | Regular issue | Vol 23, No. 4, 1985, pp.799-802
Published online, 1st January, 1970
DOI: 10.3987/R-1985-04-0799
Convenient Phase Transfer N-Arylation of 1,3-Dihydro-1,5-benzodiazepin-2-ones

El Mokhtar Essassi,* Moussa Salem, Rachid Zniber, Philippe Viallefont, and Roger Gallo

*Laboratoire de Chimie des Plantes et de Sythese Organique et Bioorganique, Faculté des Sciences, Universite Mohammed V, P.B. 1014 Rabat-RP, Morocco

Abstract

The application of phase transfer catalysis to the N-arylation of heterocyclic molecules is described ; N-arylbenzadiazepines are prepared according to this method. The phase transfer technique is compared to conventional procedures. The dynamic stereochemistry of the ring is evidenced by the change in 1Hnmr spectra line.