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Report | Regular issue | Vol 23, No. 3, 1985, pp.593-602
Published online, 1st January, 1970
DOI: 10.3987/R-1985-03-0593
On the Synthesis of (±)-Mesembranone by the Dissolving Metal Reduction of 4-Aryl-4-aminoethylcyclohexenones. Isolation of N-Methyl-5-(3’,4’-dimethoxyphenyl)-2-azabiocyclo[3.3.1]nonan-8-one

Ignacio H. Sánchez,* María Larraza, Humbert J. Flores, Eduardo Díaz, and Krzysztof Jankowski

*Facultad de Química, Universidad Nacional Autónama de México, Circuito Exterior, Ciudad Universitaria, Coyoacán 04510, Mexico


The novel 2-azabicyclo[3.3.1]nonan-8-one derivative 4 has been isolated as byproduct in the synthesis of (±)-mesembranone (2) by the dissolving metal reduction of the 4-aryl-4-aminoethylcyclohexenone 1.