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Report | Regular issue | Vol 20, No. 10, 1983, pp.1993-1999
Published online, 1st January, 1970
DOI: 10.3987/R-1983-10-1993
Synthesis of Some 3-Arylimino-5-(N-4-methoxybenzylidenehydrazono)-1,2,4-dithiazolidines

Mohammad Ramzan Ali, Rajendra Singh, and Vinay Kumar Verma

*Department of Applied Chemistry, Institute of Technology, Banaras Hindu University, Varanasi-221 005, India


A simple and convenient synthesis of some 3-arylimino-5-(N-4-methoxybenzylidenehydrazono)-1,2,4-dithiazolidines (IV a-e) has been achieved by oxidative debenzylation and cyclization of the corresponding 5-aryl-1-(4-methoxybenzylideneamino)-2-S-benzyliso-2,4-dithiobiurets (III a-e) which in turn were prepared by the condensation of certain potentially active S-benzyliso-4-methoxybenzylidenethiosemicarbazone (II) with appropriate aryl isothiocyanate. These dithiazolidines have been characterized by their synthesis through alternative routes (Scheme 1), elemental analyses and also by ir spectra.