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Report | Regular issue | Vol 19, No. 11, 1982, pp.2093-2098
Published online, 1st January, 1970
DOI: 10.3987/R-1982-11-2093
Triethylamine Solubilised Phosphorous Pentasulphide as Thiation Reagent: A Novel Route to Totally Thiated Heterocycles

Bhabagrahi Dash, E. Khalli Dora, and Chandra Sekhar Panda

*Department of Chemistry, Berhampur University, Berhampur-760 007, Orissa, India

Abstract

Triethylamine solubilised phosphorous pentasulphide (P4S10) has been evolved as the thiation agent in heterocycles such as substituted benzoxazin-4-ones, 2-pyrazolin-4-ones and pyrimidine-2,5-dione derivatives. The simple and convenient operation involving stirring (24 h) of the reaction mixture at room temperature results in the isolation of the desired products in quantitative yield.