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Note | Regular issue | Vol 51, No. 10, 1999, pp.2479-2483
Published online, 1st January, 1970
DOI: 10.3987/COM-99-8668
Synthesis of 4-Benzyl-5-(2,6-dichloro- phenyl)-2-ethoxy-1,2,3,4-tetrahydro-1,4,6,2-oxadiazaphosphorine 2-Oxide

Wynona Johnson,* Alan Faux, and Gary Fallon

*CSIRO, Molecular Science, Praivate BAg 10, Clayton South MDC, Victoria, 3169, Australia

Abstract

A derivative of the novel heterocyclic ring system - 1,2,3,4-tetrahydro-1,4,6,2-oxadiazaphosphorine (1), was prepared by the cycloaddition of the nitrile oxide generated from hydroximoyl chloride (2) with aminomethylphosphonate (3). The structure was elucidated by NMR analysis and X-Ray crystallography. The stability of the new ring system was investigated.