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Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Communication | Special issue | Vol 47, No. 1, 1998, pp.157-161
Published online, 1st January, 1970■ Total Syntheses of (-)-Polyoxin J and (-)-Polyoxin L
Published online, 1st January, 1970
DOI: 10.3987/COM-97-S(N)59
■ Total Syntheses of (-)-Polyoxin J and (-)-Polyoxin L
Hiroyuki Akita,* Kimio Uchida, and Keisuke Kato
*School of Pharmaceutical Sciences, Toho University, 2-2-1, Miyama, Funabashi, Chiba 274-8510, Japan
Abstract
A convenient synthesis of the N-protected L-carbamoylpolyoxamic acid derivative (7) from 4-O-tert-butyldiphenylsilyl-2,3-isopropylidene-L-threose (8) using vinylmagnesium bromide and its application to the total syntheses of the peptidyl nucleoside antibiotics, polyoxins J (1) and L (2), are described.
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