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Communication | Special issue | Vol 47, No. 1, 1998, pp.111-112
Published online, 1st January, 1970
DOI: 10.3987/COM-97-S(N)37
Novel Oxepane Formation by Reductive Cleavage of 1-Methoxymethyl-6,8- dioxabicyclo[3.2.1]octanes

Kenshu Fujiwara,* Akira Amano, Tetsuo Tokiwano, and Akio Murai*

*Division of Chemistry, Graduate School of Science, Hokkaido University, Sapporo 060-0810, Japan


The introduction of a methoxymethyl group at the C1 position in the 6,8-dioxabicyclo[3.2.1]octane system enabled novel formation of oxepane in reductive cleavage induced by triethylsilane and titanium(IV) chloride.