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Communication | Special issue | Vol 42, No. 1, 1996, pp.47-51
Published online, 1st January, 1970
DOI: 10.3987/COM-95-S11
Preparation of Novel Cyclic Hypervalent Idoine(III) Compounds Having Azido, Cyano, and Nitrato Ligands

Shuji Akai, Takayuki Okuno, Masahiro Egi, Takeshi Takada, Hirofumi Tohma, and Yasuyuki Kita

*Faculty of Pharmaceutical Sciences, Osaka University, 1-6 Yamadaoka, Toyonaka, Osaka 560-0043, Japan


The title cyclic hypervalent iodine compounds (4-8) were prepared in good yields by the ligand exchange reaction of the acetoxy cyclic iodinanes (1-3) with trimethylsilyl compounds and of the chloro cyclic iodinane (9) with silver nitrate, and were found to be air-stable at room temperature.