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Paper | Regular issue | Vol 43, No. 1, 1996, pp.151-172
Published online, 1st January, 1970
DOI: 10.3987/COM-95-7248
Aryl Diazinyl Ketoximes: Synthesis and Configurational Assignment

Gottfried Heinisch, Wolfgang Holzer, Thierry Langer, and Peter Lukavsky

*Institute of Pharmaceutical Chemistry, University of Innsbruck, Innrain 52a, A-6020 Innsbruck, Austria

Abstract

Preparation of a series of new aryl diazinyl ketoximes (7a,b - 12a,b) required as synthetic building blocks is described. Separation of the E/Z-isomers obtained was achieved by means of chromatography, their configuration was assigned using nmr techniques. Moreover, procedures for the synthesis of the starting ketones (1b - 6b) are given.