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Communication | Regular issue | Vol 41, No. 4, 1995, pp.661-664
Published online, 1st January, 1970
DOI: 10.3987/COM-94-7015
INOC Reaction in Alkaloid Synthesis –- Preparation of Potential Intermediate for the Synthesis of (-)-Reserpine –-

Masahiro Toyota, Masaki Matsuura, and Keiichiro Fukumoto

*Pharmaceutical Institute, Tohoku University, Aobayama, Sendai 980-77, Japan

Abstract

Intramolecular nitrile oxide cycloaddition (INOC) reaction of the nitro olefin (10) furnished the isoxazoline (11), potential synthon for the E ring segment of (-)-reserpine (1), in quantitative yield.