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Communication | Special issue | Vol 37, No. 1, 1994, pp.245-248
Published online, 1st January, 1970
DOI: 10.3987/COM-93-S47
Synthesis of 7-Azabicyclo[2.2.1]heptane and 8-Azabicyclo[3.2.1]octane Systems Using Radical Cyclization

Tatsunori Sato, Tomiyo Mori, Tadakatsu Sugiyama, Hiroyuki Ishibashi, and Masazumi Ikeda*

*Kyoto Pharmaceutical University, Misasagi, Yamashina, Kyoto 607-8414, Japan


A new method for the synthesis of the titled systems using cyclization of the α-acylamino radicals generated from methyl N-(o-bromobenzoyl)-2-(prop-2-enyl)pyrrolidine-2-carboxylates and the piperidine congener by Bu3SnH-mediated radical translocation reaction is described.