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Communication | Regular issue | Vol 38, No. 1, 1994, pp.51-54
Published online, 1st January, 1970
DOI: 10.3987/COM-93-6576
■ A Synthesis and Structural Confirmation of 3,5-Bis(2-alkylimidazol-4-yl)-1,2,4-trithiolanes

Kuniaki Tatsuta,* Shozo Miura, Naoki Kano, and Shigeo Fujita

*Graduate School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan

Abstract

The structures of the 4-formylimidazole equivalents which were prepared by heating 2-alkyl-4-dithiocarboxylimidazoles with 47% HBr or conc. H2SO4 have been revised to be 3,5-bis(2-alkylimidazol-4-yl)-1,2,4-trithiolanes by X-ray crystallographic analyses.