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Paper | Regular issue | Vol 32, No. 7, 1991, pp.1307-1315
Published online, 1st January, 1970
DOI: 10.3987/COM-91-5735
New Synthetic Derivatives of Aconitine, Delphonine and N-Deacetyllappaconitine

Samir A. Ross and S. William Pelletier*

*Institute for Natural Products Research, School of Chemical Sciences, The University of Georgia, Chemistry Building, Athens, Georgia 30602-2556, U.S.A.

Abstract

This paper reports the synthesis and spectral data for 3,13-diacetylaconitine (3), 3,13,15-triacetylaconitine (4), 3,13-diacetyl-14-benzoylaconine (7), aconine pentaacetate (10), delphonine methiodide (11), 8,9-diacetyllappaconitine (12), N-deacetyl-N-methyllappaconitine (13), N-deacetyl-N-N-dimethyllappaconitine (14), N-deacetyl-N-benzoyllappaconitine (15), N-deacetyl-N-o-anisoyllappaconitine (16), N-deacetyl-N-p-anisoyllappaconitine (17), N-deacetyl-N-(3,4,5-trimethoxybenzoyl)lappaconitine (18), N-deacetyl-N-p-nitrobenzoyllappaconitine (19), N-deacetyl-N-triphenylmethyllappaconitine (20), and N-deacetyl-N-(3,3-dimethylacryloyl)lappaconitine (21).