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Communication | Special issue | Vol 30, No. 1, 1990, pp.381-384
Published online, 1st January, 1970
DOI: 10.3987/COM-89-S85
Chiral Synthesis of the Intermediate of Atisine

Masataka Ihara, Makoto Suzuki, and Keiichiro Fukumoto*

*Pharmaceutical Institute, Tohoku University, Aobayama, Sendai 980-8578, Japan


The chiral key intermediate, (+)-(1R,5R)-3-benzyl-1-methoxymethyloxymethyl-5-methyl-9-methylene-3-azabicyclo[3.3.1]nonane (2), for the synthesis of atisine (5) was prepared from dimethyl 3-benzyl-3-azabicyclo[3.3.1]nonan-9-one-1,5-dicarboxylate (6) by a chemical methodology.