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Communication | Special issue | Vol 30, No. 1, 1990, pp.335-337
Published online, 1st January, 1970
DOI: 10.3987/COM-89-S60
A New Synthesi of (±)-Chilenamine, an Isoindolobenzazepine Alkaloid

Shingo Yasuda, Yu-ichi Sugimoto, Chisato Mukai, and Miyoji Hanaoka*

*Faculty of Pharmaceutical Scicences, Kanazawa University, 13-1 Takara-machi, Kanazawa 920-0934, Japan

Abstract

(±)-Chilenamine (1), an isoindolobenzazepine alkaloid, was efficiently synthesized starting from 6-bromo-2,3-dimethoxybenzaldehyde (5) and 3,4-methylenedioxyphenethylamine (6) via the N-substituted benzazepine (10) by radical cyclization.