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Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Communication | Regular issue | Vol 29, No. 5, 1989, pp.841-845
Published online, 1st January, 1970■ Formation of Thiocyanates by Ring Cleavage from 2-Imino-5,6-dihydro-4H-1,3-thiazine
Published online, 1st January, 1970
DOI: 10.3987/COM-89-4867
■ Formation of Thiocyanates by Ring Cleavage from 2-Imino-5,6-dihydro-4H-1,3-thiazine
Mitsuhiro Ichinari and Yoshio Hayase
*Aburahi Laboratories, Shionogi & Co. Ltd., Gotanda, Koka-cho, Koka-gun, Shiga 520-3423, Japan
Abstract
The reaction of 2-imino-5,6-dihydro-4H-1,3-thiazine with diethyl chlorophosphate, diethyl chlorothiophosphate and p-toluenesulfonyl chloride in the presence of base gave N-propylthiocyanate derivatives of diethyl phosphoramide, diethyl phosphorothioamide and p-toluenesulfonamide, respectively, in goad yield.
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