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Zenichi Yoshida (1925-2023)
Zenichi Yoshida (1925-2023)
Professor. Zenichi Yoshida,
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Paper | Regular issue | Vol 27, No. 7, 1988, pp.1679-1684
Published online, 1st January, 1970■ Metalation Reactions. XII. One-pot Synthesis of 1,3-Benzothiasiloles, 1,3-Benzothiastannoles and 1,3-Benzodithioles
Published online, 1st January, 1970
DOI: 10.3987/COM-88-4551
■ Metalation Reactions. XII. One-pot Synthesis of 1,3-Benzothiasiloles, 1,3-Benzothiastannoles and 1,3-Benzodithioles
Salvatore Cabiddu,* Claudia Fattuoni, Costantino Floris, and Gioanna Gelli
*Istituto di Chimica Organica, Università di Cagliari, Via Ospedale 72, I-09124 Cagliari, Italy
Abstract
The dilithiated species of (methylthio)benzene reacts with various dichlorosilanes, dichlorostannanes and sulfur chloride yielding derivatives of 1,3-benzothiasilole, 1,3-benzothiastannole and 1,3-benzodithiole respectively. By reaction with tetrachlorosilane a spirocyclic silicon compound is obtained. A description of the synthesis is given. The structures of the reaction products were determined by elemental and spectroscopic analyses.
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