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Obituary
Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Communication | Special issue | Vol 76, No. 2, 2008, pp.1069-1074
Published online, 19th June, 2008■ Stereoselective Synthesis of Maitotoxin GHI-Ring System Having a 1,2-Diol Side Chain
Published online, 19th June, 2008
DOI: 10.3987/COM-08-S(N)113
■ Stereoselective Synthesis of Maitotoxin GHI-Ring System Having a 1,2-Diol Side Chain
Masanori Nagatomo and Tadashi Nakata*
*Department of Chemistry, Faculty of Science, Tokyo University of Science, 1-3 Kagurazaka, Shinjuku-ku, Tokyo 162-8601, Japan
Abstract
The stereoselective synthesis of maitotoxin GHI-ring system having a 1,2-diol side chain was accomplished via successive SmI2-induced reductive cyclizations of β-alkoxyacrylate-aldehyde and optically active (E)-β-alkoxyvinylsulfoxide-aldehyde, dihydroxylation of α,β-unsaturated δ-lactone, and Sharpless asymmetric dihydroxylation of the side chain.
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