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Paper | Regular issue | Vol 71, No. 10, 2007, pp.2173-2181
Published online, 20th July, 2007
DOI: 10.3987/COM-07-11098
Synthesis and Characterization of Some Fused Tricyclic Spermidine Derivatives of Cyclotriphosphazene

Hanife Ibisoglu

*Department of Chemistry, Gebze Institute of Technology, Gebze 41400, Kocaeli, Turkey

Abstract

A number of derivatives of 6-chloro-2, 2-X2-1, 3, 5, 7, 11, 16-hexa aza-4,6-diphosphatricyclohexadeca-2, 4, 6-triene {X=SPh, [OCH2(CF2)2CH2O]0.5, pyr, NMe2, NHPrn, Ph, NHBut} have been synthesised using two different reaction routes (1, 2) giving rise to penta-substituted-mono-chloro-compounds. The remaining chlorine atom in these products was reluctant to react with neutral nitrogen nucleophiles. The structures of the compounds were determined by elemental analysis, mass spectrometry and by 1H and 31P-NMR spectrocsopy.