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Obituary
Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Paper | Regular issue | Vol 71, No. 3, 2007, pp.531-542
Published online, 26th January, 2007■ Diastereoselective Synthesis of Spiro-β-lactams via Staudinger Reaction
Published online, 26th January, 2007
DOI: 10.3987/COM-06-10942
■ Diastereoselective Synthesis of Spiro-β-lactams via Staudinger Reaction
Susana Rojas-Lima,* Lidia Santillán-Sid, Heraclio López-Ruiz, and Alejandro Álvarez-Hernández
*Chemical Research Center (CIQ), Autonomous University of Hidalgo (UAEH) University City, Pachuca-Tulancingo road Km 4.5, Pachuca de Soto, Hidalgo, CP 42076, México
Abstract
In this work, eleven new spiro-β-lactams have been prepared using the Staudinger reaction of isomaleimides (1a-d) and carboxylic acids (chloroacetic acid, (-)-menthoxyacetic acid (7) and an oxazolidinone derived acid (10)) in the presence of triphosgene under mild condition. All reactions have been shown to be stereoselective. The new stereogenic centers were assigned by X-ray diffraction.
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