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Note | Special issue | Vol 67, No. 2, 2006, pp.785-790
Published online, 8th November, 2005
DOI: 10.3987/COM-05-S(T)62
Synthesis and Spectral Properties of Azaterrylene Dicarboximide Derivative

Yukinori Nagao, Yuko Ogihara, Masafumi Adachi,* and Kozo Kozawa

*Department of Industrial Chemistry, Faculty of Science and Technology, Science University of Tokyo, 2641 Yamazaki, Noda, Chiba 278-8510, Japan

Abstract

Azaterrylene dicarboximide derivative was prepared by the coupling of N-pentyl-9-tributylstannylperylene-1,8-dicarboximide with 5-bromo-1,8-dimethylisoquinoline in the presence of Pd(PPh3)4 and following ring closure reaction by using t-BuOK/DBN. Spectral properties in solution were investigated and analyzed by molecular orbital method.