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Obituary
Yoshito Kishi (1937-2023)
Yoshito Kishi (1937-2023)
Professor. Yoshito Kishi,
a member of the Honorary Editorial Associates of HETEROCYCLES,
has passed away on January 9, 2023 at the age of 85.
I deeply express my regret over his death.
Kunio Ogasawara
Editor
January 13, 2023
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Paper | Regular issue | Vol 65, No. 8, 2005, pp.1843-1856
Published online, 17th May, 2005■ Selective Reduction of Nitrocinnamoylfumagillols with α,β-Unsaturated Ester Using Borohydride Exchange Resin (BER)-Nickel Acetate
Published online, 17th May, 2005
DOI: 10.3987/COM-05-10425
■ Selective Reduction of Nitrocinnamoylfumagillols with α,β-Unsaturated Ester Using Borohydride Exchange Resin (BER)-Nickel Acetate
Hong Woo Lee,* Joong Bok Ahn, Jung Hwa Lee, Sung Kwon Kang, Soon Kil Ahn, and Sang Joon Lee
*Chemical Process Development Laboratories, Chong Kun Dang Research Institute, Chonan P.O. Box 74, Chonan, 330-831, Korea
Abstract
Borohydride Exchange Resin (BER) — nickel acetate system readily reduces nitrocinnamoylfumagillols to the corresponding amines in excellent yields, high chemoselectivity, and simple procedure. Especially, this system tolerates two epoxides (spiro-epoxide and the one on C4 alkene side chain) and the α,β-unsaturated ester moiety at C6 on the fumagillol.
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