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Paper | Special issue | Vol 64, No. 1, 2004, pp.75-91
Published online, 26th January, 2004
DOI: 10.3987/COM-03-S(P)1
Synthetic Study of Hydrophilic Analogue of Scyphostatin via π-Facial Selective Diels-Alder Reaction

Wataru Miyanaga, Ryukichi Takagi, and Katsuo Ohkata*

*Department of Chemistry, Faculty of Science, Hiroshima University, 1-3-1 Kagamiyama, Higashi-Hiroshima, Hiroshima 739-8526, Japan


An analogue of the hydrophilic moiety of scyphostatin was synthesized via π-facial selective Diels-Alder reaction of a 2,5-cyclohexadien-1-one bearing a spirolactone with cyclopentadiene.