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Note | Regular issue | Vol 60, No. 11, 2003, pp.2535-2542
Published online, 5th September, 2003
DOI: 10.3987/COM-03-9866
■ Synthesis and Characterization of a New Metal-free Azaphthalocyanine Containing Four Peripheral Ion Jacks

Xiguang Du,* Chunyu Ma, Xiaoke Hou, Gui Wang, Wancheng Li, and Guotong Du*

*Laboratory of Organic Synthesis, Department of Chemistry, Northeast Normal University, Changchun, 130024, China

Abstract

A synthesis of a new 1,10-phenanthroline-appended metal-free azaphthalocyanine(azaPc), which is generated from precursor, 10,12-diimino-11 H-pyrrolo[3,4-b]dipyrido[3,2-f:2’,3’-h]quinoxaline, is described. This azaPc is purified by absolute methanol in a Soxlet apparatus, then under high vacuum (10-4Pa) and is unequivocally characterized by its elemental analysis and spectrometry.