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Communication | Regular issue | Vol 53, No. 6, 2000, pp.1239-1245
Published online, 1st January, 1970
DOI: 10.3987/COM-00-8873
Synthesis of Novel Macrocyclic Compounds Utilizing Characteristic Bonding Properties of Hypervalent Sulfur

Noboru Matsumura,* Tsunao Konishi, Hirokazu Hayashi, Masanori Yasui, Fujiko Iwasaki, and Kazuhiko Mizuno

*Department of Applied Chemistry, College of Engineering, Osaka Prefecture University, Sakai, Osaka 599-8531, Japan

Abstract

The convenient method for the synthesis of 18-, 26-, and 30-membered macrocyclic compounds by utilizing the characteristic bonding properties of the hypervalent sulfur in the 10-S-3 tetraazathiapentalene derivatives and their chemical properties have been described. The structures were established by their spectral data and X-Ray crystallographic analysis.